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CN-117323947-B - Octenyl succinic acid modified porous starch ester supported naringin compound preparation device

CN117323947BCN 117323947 BCN117323947 BCN 117323947BCN-117323947-B

Abstract

The invention relates to the technical field of medical health-care food, and particularly discloses a preparation device of an octenyl succinic acid modified porous starch ester supported naringin compound, which comprises a preparation liquid ultrasonic mixing cylinder assembly, wherein a mixing top cover assembly is arranged at the top of the preparation liquid ultrasonic mixing cylinder assembly, and a mixing liquid shaking and stirring assembly is arranged on the mixing top cover assembly; the bottom of the preparation liquid ultrasonic mixing cylinder assembly is rotatably provided with a rocker arm base assembly, both sides of the top of the preparation liquid ultrasonic mixing cylinder assembly are fixedly provided with preparation liquid mixing cylinder assemblies, the preparation liquid ultrasonic mixing cylinder assemblies comprise preparation liquid ultrasonic mixing cylinders, a plurality of mixing cylinder bottom arm platforms are fixedly arranged on the preparation liquid ultrasonic mixing cylinders through reinforcing ribs, bottom arm platform main shafts are fixedly arranged on the mixing cylinder bottom arm platforms, the bottom end of the inside of the preparation liquid ultrasonic mixing cylinder is fixedly provided with an aerator pipe, and the outer side of the bottom of the preparation liquid ultrasonic mixing cylinder is fixedly provided with a liquid suction pump. The invention has the characteristic of full mixing.

Inventors

  • LU SHENGMIN
  • WANG LU
  • ZHENG MEIYU
  • CAO FENG
  • YANG YING

Assignees

  • 浙江省农业科学院

Dates

Publication Date
20260508
Application Date
20220512

Claims (8)

  1. 1. The preparation device of the octenyl succinic acid modified porous starch ester supported naringin compound is characterized by comprising a preparation liquid ultrasonic mixing cylinder assembly (100), wherein a mixing top cover assembly (200) is arranged at the top of the preparation liquid ultrasonic mixing cylinder assembly (100), a mixed liquid shaking stirring assembly (400) is arranged on the mixing top cover assembly (200), a rocker arm base assembly (300) is rotatably arranged at the bottom of the preparation liquid ultrasonic mixing cylinder assembly (100), preparation liquid mixing cylinder assemblies (500) are fixedly arranged on two sides of the top of the preparation liquid ultrasonic mixing cylinder assembly (100), the preparation liquid ultrasonic mixing cylinder assembly (100) comprises a preparation liquid ultrasonic mixing cylinder (101), a plurality of mixing cylinder bottom arm platforms (102) are fixedly arranged on the preparation liquid ultrasonic mixing cylinder (101) through reinforcing ribs (103), a bottom arm platform main shaft lever (104) is fixedly arranged on the mixing cylinder bottom arm platform (102), an aerator pipe (105) is fixedly arranged at the bottom end inside the preparation liquid ultrasonic mixing cylinder (101), and a liquid suction pump (106) is fixedly arranged on the outer side of the bottom of the preparation liquid ultrasonic mixing cylinder (101); The rocker arm base assembly (300) comprises a ring-shaped rocker arm base stand (301), a plurality of rocker arm side tables (302) are symmetrically and fixedly arranged on the edge of the ring-shaped rocker arm base stand (301), stand supporting legs (303) are fixedly arranged at the bottoms of the rocker arm side tables (302), a first fixed disc (305) is fixedly arranged inside the ring-shaped rocker arm base stand (301) through a first supporting rod (304), a driving motor (306) is fixedly arranged at the bottom of the first fixed disc (305), a second fixed disc (308) is fixedly arranged on a shaft rod of the driving motor (306), and a ring-shaped central gear (307) is fixedly arranged outside the second fixed disc (308) through a second supporting rod (309); The rocker arm side table (302) is characterized in that a rotating main arm shaft lever (310) is rotatably arranged at the top of the rocker arm side table (302) through a bearing seat, a supporting arm (311) is fixedly arranged at the top of the rotating main arm shaft lever (310), a distal arm body end of the supporting arm (311) is rotatably connected with the bottom of a bottom arm table main shaft lever (104) through the bearing seat, a driven gear (312) is fixedly arranged in the middle of the rotating main arm shaft lever (310), and the driven gear (312) is meshed with a ring-shaped central gear (307).
  2. 2. The preparation device of octenyl succinic acid modified porous starch ester supported naringin complex according to claim 1, wherein the mixing top cover assembly (200) comprises a mixing top cover (201), a top cover spray pipe (206) is fixedly arranged inside the mixing top cover (201), a top cover plate (202), a gas release pipe (208) and a top cover center ball seat (207) are fixedly arranged at the top of the mixing top cover (201), a top cover driving motor (203) is fixedly arranged at the top of the top cover plate (202), and an inclined holding pipe (205) is fixedly arranged on a shaft rod of the top cover driving motor (203) through a supporting side plate (204).
  3. 3. The preparation device of the octenyl succinic acid modified porous starch ester supported naringin complex according to claim 2, wherein the mixed liquor shaking stirring assembly (400) comprises a mixed liquor shaking stirring rod (401), a shaking ball head (402) is fixedly arranged at the top of the mixed liquor shaking stirring rod (401), a mixed liquor shaking stirring support rod (403) and an ultrasonic generator (404) are fixedly arranged at the bottom of the mixed liquor shaking stirring rod (401), and a top arm rod of the mixed liquor shaking stirring rod (401) is sleeved in an inclined holding tube (205).
  4. 4. The preparation device of the octenyl succinic acid modified porous starch ester supported naringin complex as claimed in claim 1, wherein the preparation liquid mixing barrel assembly (500) comprises a preparation liquid mixing barrel (501), a charging hopper (507) and a preparation liquid outlet bottom pipe (502) are respectively and fixedly arranged at the top and the bottom of the preparation liquid mixing barrel (501), a buckling cover (508) and an electromagnetic metering valve (503) are respectively arranged on the charging hopper (507) and the preparation liquid outlet bottom pipe (502), a preparation liquid mixing barrel stirring motor (506) is fixedly arranged at one side of the top of the preparation liquid mixing barrel (501), a preparation liquid mixing barrel stirring strut (510) is fixedly arranged on a preparation liquid mixing barrel stirring shaft lever (509) of the preparation liquid mixing barrel stirring motor (506), and an air pressure vent pipe (504) and a preparation liquid mixing barrel high pressure flushing pipe (505) are respectively and fixedly arranged at two ends of the inner side of the top of the preparation liquid mixing barrel (501).
  5. 5. The preparation device of the octenyl succinic acid modified porous starch ester supported naringin complex as claimed in claim 3, wherein the rocking ball head (402) moves in the top cover center ball seat table (207) in an omnibearing manner, and the top cover center ball seat table (207) and the top cover driving motor (203) are coaxial in axis.
  6. 6. The octenyl succinic acid modified porous starch ester supported naringin complex preparation device according to claim 1, wherein a plurality of support arms (311) are located between the preparation liquid ultrasonic mixing cylinder (101) and the annular rocker arm base stand (301), and the plurality of support arms (311) are distributed in parallel structure.
  7. 7. The preparation device of the octenyl succinic acid modified porous starch ester supported naringin compound according to claim 1, wherein two groups of preparation liquid mixing cylinder assemblies (500) at the top of the preparation liquid ultrasonic mixing cylinder assembly (100) are respectively used as naringin dissolving cylinder and octenyl succinic acid porous starch mixing cylinder; the preparation method of the octenyl succinic acid modified porous starch ester supported naringin compound comprises the following steps, (S01) dissolving a proper amount of naringin in a solvent I to prepare a solution A; (S02) adding a proper amount of octenyl succinic acid porous starch into the solvent II, dispersing and mixing to prepare a suspension B; (S03) placing the solution A in the step (S01) and the suspension B in the step (S02) into an ultrasonic mixing device for ultrasonic mixing, and centrifuging and drying to obtain the octenyl succinic acid modified porous starch ester supported naringin complex.
  8. 8. The preparation device of the octenyl succinic acid modified porous starch ester supported naringin complex as claimed in claim 7, wherein the ultrasonic intensity is 10-300W, and the ultrasonic time is 15-30 min.

Description

Octenyl succinic acid modified porous starch ester supported naringin compound preparation device Technical Field The invention relates to the technical field of medical health-care foods, in particular to a preparation device of an octenyl succinic acid modified porous starch ester supported naringin compound. Background Naringin (Naringin, NA) is an important dihydrocitrus flavonoid compound which is widely used in Rutaceae plants and has various biological activities such as anti-inflammatory, antibacterial, anti-tumor and lipid-lowering, but NA has low solubility in water and is easy to decompose in saliva and gastric juice, so that the in vivo bioavailability is low, and therefore, the naringin is deprotected and carried by a proper carrier, so that the bioavailability is improved, and the application of the naringin in the fields of foods, cosmetics, medicines and the like is greatly expanded. Octenyl succinic acid modified porous starch ester (Octenyl succinate modified porous STARCH ESTER, OSAPS) is a starch-based carrier with both adsorptivity and amphipathy, which enables it to have both loading and solubilization properties, and is a well-recognized safe food additive when the degree of esterification of octenyl succinic acid is less than 3%, so that octenyl succinic acid modified porous starch ester is a potential carrier, but how to use octenyl succinic acid modified porous starch ester to load naringin remains a difficult problem. Disclosure of Invention The invention provides a fully mixed preparation device for an octenyl succinic acid modified porous starch ester supported naringin compound, which aims to solve the technical problems existing in the biological utilization process of the existing naringin. According to the technical scheme, the preparation device of the octenyl succinic acid modified porous starch ester supported naringin compound comprises a preparation liquid ultrasonic mixing cylinder assembly, a mixing top cover assembly is arranged at the top of the preparation liquid ultrasonic mixing cylinder assembly, a mixed liquid shaking and stirring assembly is arranged on the mixing top cover assembly, a rocker arm base assembly is rotatably arranged at the bottom of the preparation liquid ultrasonic mixing cylinder assembly, preparation liquid mixing cylinder assemblies are fixedly arranged on two sides of the top of the preparation liquid ultrasonic mixing cylinder assembly, the preparation liquid ultrasonic mixing cylinder assembly comprises a preparation liquid ultrasonic mixing cylinder, a plurality of mixing cylinder bottom arm platforms are fixedly arranged on the preparation liquid ultrasonic mixing cylinder through reinforcing ribs, a bottom arm platform main shaft rod is fixedly arranged on the mixing cylinder bottom arm platform, an aerator pipe is fixedly arranged at the bottom end inside the preparation liquid ultrasonic mixing cylinder, and a liquid suction pump is fixedly arranged on the outer side of the bottom of the preparation liquid ultrasonic mixing cylinder. When the ultrasonic mixed solution preparation device is used, the two sides of the top of the ultrasonic mixed solution preparation device are fixedly provided with the ultrasonic mixed solution preparation device, the two groups of ultrasonic mixed solution preparation device 0 are respectively used as naringin dissolving cylinders and octenyl succinic acid porous starch mixed cylinders, naringin and acetone are added into one group of ultrasonic mixed solution preparation device and stirred to prepare solution A, octenyl succinic acid porous starch petroleum ether is added into the other group of ultrasonic mixed solution preparation device and stirred to prepare suspension B, then the solution A and the suspension B in the two groups of ultrasonic mixed solution preparation devices are added into the ultrasonic mixed solution preparation device according to a ratio, at the moment, the top of the ultrasonic mixed solution preparation device is provided with a mixed top cover assembly, the mixed top cover assembly is provided with a mixed solution shaking stirring assembly, the bottom end of the ultrasonic mixed solution preparation device is fixedly provided with an aeration pipe, the aeration pipe is communicated with an external high-pressure air feeding tank, the upward bottom liquid in the ultrasonic mixed solution preparation device is realized through the high-pressure air feeding pipe, the upper and lower full mixing of the solution in the ultrasonic mixed solution preparation device is further ensured, and the ultrasonic mixed solution preparation device and the mixed solution preparation device is fully mixed in the mixed solution preparation device is further realized through shaking the ultrasonic mixed solution preparation device in the mixing mode of the two stages, and the ultrasonic mixed solution preparation device is further realized through shaking the vibration device. The aeration