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CN-120437028-B - Double-tube face-cleaning product with functions of removing cutin and blackheads, and preparation method and application thereof

CN120437028BCN 120437028 BCN120437028 BCN 120437028BCN-120437028-B

Abstract

The invention belongs to the technical field of cosmetics, and particularly relates to a double-tube face cleaning product with exfoliating function and a preparation method and application thereof. Specifically, the exfoliating blackhead composition, the surfactant, the preservative, the humectant, the thickener and the fatty acid are applied to a face cleaning product, and meanwhile, the face cleaning emulsion is in a double-tube form, wherein the inner tube is mainly a gel system, and the outer tube is mainly a gel system, so that the effective components in the exfoliating blackhead composition contain papaya fruit extracts, fig fermentation liquid and saccharomycetes/zinc fermentation products. The double-tube type can prevent the enzyme components from being inactivated by contacting with the surfactant components for a long time, thereby prolonging the shelf life of the product, and realizing the effects of mildly exfoliating and blackhead removing of the product, so that the double-tube type gel has good practical application value.

Inventors

  • WANG XIAONA
  • LI CHUNTING
  • NING HUI
  • GUO HAIJIAO
  • CHEN XIN
  • HAN TINGTING
  • YANG SUZHEN
  • XU PEIPEI
  • ZHANG NA
  • JI LIQIANG

Assignees

  • 山东福瑞达生物股份有限公司

Dates

Publication Date
20260512
Application Date
20250527

Claims (12)

  1. 1. The double-tube face cleaning product with the exfoliating and blackhead is characterized by comprising an outer tube material and an inner tube material; The external pipe comprises, by mass, 3-8% of a exfoliating black head composition, 5-15% of a humectant, 2-8% of a thickening agent, 0.5-1.5% of a preservative, 0.1-0.5% of a pH value regulator and the balance of water, wherein the exfoliating black head composition comprises a papaya fruit extract, a fig fermentation broth and a saccharomycete/zinc fermentation product, the mass ratio of the papaya fruit extract, the fig fermentation broth and the saccharomycete/zinc fermentation product is 1-10:1-10:1-10, and the effective components in the papaya fruit extract are papain; The inner pipe comprises, by mass, 35-55% of a surfactant, 2-5% of a thickener, 10-15% of a humectant, 0.5-1.0% of a preservative, 0.5-3% of fatty acid and the balance of water, wherein the surfactant comprises an amino acid type surfactant and a non-amino acid type surfactant, the mass ratio of the amino acid type surfactant to the non-amino acid type surfactant is 3-6:4-5, the inner pipe further comprises sodium citrate, the content of the sodium citrate is 2-4%, and the fatty acid is lauric acid; in the outer tube material, the fig fermentation liquid is prepared by the following method: Inoculating lactobacillus into liquid fermentation medium containing fructus fici powder for fermentation treatment, and filtering, sterilizing and removing impurities; Wherein the lactobacillus is lactobacillus rhamnosus CGMCC No. 27781, and the inoculation amount is controlled to be 1-5% (V/V); The fig powder is specifically obtained by drying and crushing figs and sieving the dried figs with a 40-80-mesh sieve, wherein the adding amount of the fig powder is controlled to be 1-10% (w/v, g/mL); The liquid fermentation medium also comprises a carbon source, wherein the carbon source is white sugar, and the mass volume fraction of the white sugar in the liquid fermentation medium is 1-6% (w/v, g/mL).
  2. 2. The dual tube exfoliating cleanser product of claim 1 wherein the lactobacillus, specifically lactobacillus rhamnosus CGMCC No. 27781, is controlled to an inoculum size of 3%.
  3. 3. The dual-tube cleansing product with exfoliating and blackhead according to claim 1, wherein the fig powder is obtained by drying and crushing fig and sieving the dried fig powder with a 60-mesh sieve, and the addition amount of the fig powder is controlled to be 5%.
  4. 4. The dual exfoliating, blackhead dual tube cleansing product of claim 1 wherein the white sugar is present in the liquid fermentation medium at a mass volume fraction of 4%.
  5. 5. The dual pipe exfoliating and blackhead cleansing product of claim 1 wherein the fermentation process is performed for a period of time ranging from about 24 hours to about 96 hours at a temperature ranging from about 25 ℃ to about 40 ℃; The filtration adopts ceramic membrane filtration, and the pore diameter of the ceramic membrane is 50-200nm.
  6. 6. The dual exfoliating, blackhead cleansing product of claim 1 wherein the humectant in the outer tubing is any one or more of glycerin, 1, 2-hexanediol, dipropylene glycol, methyl propylene glycol, butylene glycol, sodium hyaluronate; The thickener is any one or more of sodium polyacrylate, carbomer, xanthan gum, hydroxyethyl cellulose, polyacrylate crosslinked polymer 6, acrylamide/VP copolymer, hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer, aluminum magnesium silicate, hydroxypropyl starch phosphate, acrylic ester copolymer, PEG 120 methyl glucose dioleate and PEG 150 distearate; the preservative is any one or more of p-hydroxyacetophenone and octanoyl hydroxamic acid; the pH regulator is any one or more of tromethamine, triethanolamine and arginine.
  7. 7. The exfoliating, blackhead dual tube cleansing product of claim 1 wherein the amino acid type surfactant in the inner tube is any one or more of potassium cocoyl glycinate, potassium lauroyl glycinate, cocoyl glycinate TEA salt, sodium cocoyl glycinate, sodium lauroyl glycinate, sodium cocoyl glutamate, cocoyl glutamate TEA salt, sodium lauroyl sarcosinate, disodium cocoyl glutamate, sodium cocoyl aminopropionate, sodium methyl cocoyl taurate; The non-amino acid type surfactant is any one or more of sodium lauroyl taurate, potassium cocoyl hydrolyzed collagen, cocamidopropyl hydroxysulfobetaine and sodium lauroyl amphoacetate; the thickener is one or more of modified corn starch, hydroxypropyl starch phosphate, PEG-120 methyl glucose dioleate and sodium acrylate/sodium acryloyldimethyl taurate copolymer; The humectant is any one or two of glycerol and 1, 2-hexanediol; the preservative is any one or more of p-hydroxyacetophenone and octanoyl hydroxamic acid.
  8. 8. A method of preparing a dual tube exfoliating cleansing product according to any one of claims 1 to 7, wherein the method of preparing comprises preparing an outer tube gel formulation and an inner tube cleansing cream formulation.
  9. 9. The method of preparing the outer tube gel formulation of claim 8, comprising: S1-1, mixing, stirring and heating water, a thickening agent and a humectant to 80-85 ℃, and keeping the temperature, stirring until the mixture is completely dissolved and cooling; s1-2, adding a pH value regulator when the temperature is reduced to 45-50 ℃, and stirring, mixing and dissolving uniformly; S1-3, adding the blackhead removal composition and the preservative when the temperature is reduced to 40-45 ℃, stirring, mixing, dissolving uniformly, and discharging; the preparation method of the inner tube facial cleanser preparation comprises the following steps: s2-1, mixing a surfactant, water, a humectant, fatty acid, a thickener and sodium citrate, stirring and heating to 90-95 ℃, keeping the temperature and stirring until the mixture is completely dissolved, and cooling after keeping the temperature for 30-40 min; s2-2, when the temperature is reduced to 45-50 ℃, adding a humectant and a preservative, uniformly dispersing/dissolving, preserving heat, stirring for 10-15 min, and discharging.
  10. 10. The preparation method of claim 9, further comprising filling the outer tube gel preparation and the inner tube facial cleanser preparation in a container, wherein the mass ratio of the outer tube gel to the inner tube facial cleanser is 0.5-5:1.
  11. 11. Use of a product according to any one of claims 1 to 7 for the preparation of exfoliating and blackhead cosmetics.
  12. 12. A exfoliating, blackhead cosmetic product, characterized in that it comprises a product according to any one of claims 1 to 7.

Description

Double-tube face-cleaning product with functions of removing cutin and blackheads, and preparation method and application thereof Technical Field The invention belongs to the technical field of cosmetics, and particularly relates to a double-tube face cleaning product with exfoliating function and a preparation method and application thereof. Background The disclosure of this background section is only intended to increase the understanding of the general background of the invention and is not necessarily to be construed as an admission or any form of suggestion that this information forms the prior art already known to those of ordinary skill in the art. The skin cuticle is the final product of the differentiation of the epidermal keratinocyte, is positioned at the outermost layer of the skin, is a pioneer guard against the external stimulus first line, plays a role of a barrier, protects the body from the influence of severe environmental factors, limits the loss of moisture and prevents the entry of external microorganisms or compounds. If the metabolism of the horny layer is too slow, horny cells are excessively piled up to make the horny layer thicker. The excessive thickness of the horny layer not only inhibits the generation of new horny cells, but also influences the penetration and absorption of skin to moisture and skin care products, so that the skin becomes dry, dull, rough and hard, and even the formation of skin problems such as skin acne, mao Zhoujiao and the like can be aggravated. The skin is required to properly manage the cutin metabolic process, on the one hand, the skin is helped to remove redundant cutin, so that the skin is smoother, finer and brighter, and on the other hand, the skin barrier is prevented from being damaged by excessive cutin removal, so that the cutin removal product becomes a focus of attention of the cosmetic and skin health industry. The inventor finds that the common components mainly comprise salicylic acid, fruit acid and the like, have good exfoliating effect, but have lower pH value and certain irritation, and are easy to excessively exfoliate and destroy skin barrier if used improperly. In addition, blackheads, also known as comedones, are open comedones, and are currently widely known as a "plug" sample consisting of sebum, cell debris, and bacteria. The formation process is that excessive grease is accumulated in pores, the pores are squeezed more and more, the grease is wrapped on skin to become white comedones, the skin is broken to become black when the skin is oxidized by air, and the black comedones are formed, so that the acne is more serious. At present, a plurality of blackhead removing products are sold in the market, and the blackhead removing effect is uneven. The inventor finds that the traditional blackhead removing product basically adopts a strong acid system such as azelaic acid and the like to develop products, and has great product irritation. Face cleansing is the first step in skin care, which begins with face washing. Therefore, there is a need to develop a mild and effective exfoliating and exfoliating cleansing product for improving the skin problems of consumers such as excessive horny layer, facial blackness, etc., and achieving skin care effect when consumers wash their faces. Disclosure of Invention Aiming at the defects existing in the prior art, the invention aims to provide a double-tube facial cleanser with exfoliating and blackhead, and a preparation method and application thereof. Specifically, the exfoliating blackhead composition, the surfactant, the preservative, the humectant, the thickener and the fatty acid are applied to a face cleaning product, and meanwhile, the face cleaning emulsion is in a double-tube form, wherein the inner tube is mainly a gel system, and the outer tube is mainly a gel system, so that the effective components in the exfoliating blackhead composition contain papaya fruit extracts, fig fermentation liquid and saccharomycetes/zinc fermentation products. The double-tube type can prevent the enzyme component from being inactivated by contacting with the surfactant component for a long time, thereby prolonging the shelf life of the product and realizing the effects of mildly removing cutin and blackhead of the product. Based on the above results, the present invention has been completed. In order to achieve the technical purpose, the technical scheme provided by the invention is as follows: in a first aspect of the invention, there is provided a dual tube cleansing product having exfoliating, blackhead, the cleansing product comprising an outer tube material and an inner tube material; The external pipe comprises, by mass, 3-8% of a exfoliating black head composition, 5-15% of a humectant, 2-8% of a thickening agent, 0.5-1.5% of a preservative, 0.1-0.5% of a pH value regulator and the balance of water, wherein the exfoliating black head composition comprises, by mass, a papaya fruit extract, a fig f