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CN-121971325-A - Oil tea seed oil diglyceride composition capable of relieving, removing wrinkles, removing black and improving eyesight, eye mask and preparation method thereof

CN121971325ACN 121971325 ACN121971325 ACN 121971325ACN-121971325-A

Abstract

The invention discloses a camellia seed oil diglyceride composition for relieving, removing wrinkles, removing black and improving eyesight, an eye mask and a preparation method thereof, and relates to the technical field of eye masks. The camellia seed oil diglyceride composition comprises the following raw materials of camellia seed oil diglyceride, a cynanchum atratum extract, a tremella fruit body extract, a kava root extract, a gynostemma pentaphylla extract, a cornflower extract and a purslane extract. The camellia seed oil diglyceride composition disclosed by the invention can realize four effects of relieving and repairing, resisting wrinkle and lightening, removing black and improving eyesight and protecting eyes in a synergistic manner under specific components and proportions, and is mild and free of irritation and meets the eye care requirements of multiple skin types.

Inventors

  • CHEN KAI
  • CHENG JIANQIANG
  • CHEN XIAOLEI
  • Zhan Zhenkun
  • YU WEIMING

Assignees

  • 广东善百年特医食品有限公司

Dates

Publication Date
20260505
Application Date
20260402

Claims (10)

  1. 1. A composition of oil tea seed oil diglyceride for relieving, removing wrinkles, removing black and improving eyesight is characterized by comprising the following raw materials of oil tea seed oil diglyceride, cynanchum atratum extract, tremella fruit body extract, kava root extract, gynostemma pentaphylla extract, cornflower extract and purslane extract.
  2. 2. The camellia seed oil diglyceride composition according to claim 1, which comprises, by mass, 1-10 parts of camellia seed oil diglyceride, 2-5 parts of cynanchum atratum extract, 3-6 parts of tremella fruit body extract, 1-3 parts of kava root extract, 2-6 parts of gynostemma pentaphylla extract, 2-5 parts of cornflower extract and 2-6 parts of purslane extract.
  3. 3. The camellia seed oil diglyceride composition according to claim 1, wherein the preparation method of the camellia seed oil diglyceride comprises the following steps: (1) Mixing oil tea seed oil, a solvent and an enzyme A, and performing primary enzymolysis to obtain a product 1; (2) And mixing the product 1 with enzyme B, performing secondary enzymolysis, filtering, centrifuging, and purifying by molecular distillation to obtain the oil tea seed oil diglyceride.
  4. 4. The camellia seed oil diglyceride composition according to claim 3, wherein in the step (1), the solvent is glycerin, propylene glycol and water in a mass ratio of 0.06-0.09:0.3-0.5:1, the enzyme A is a mixture of candida antarctica lipase and pseudomonas cepacia lipase, and in the step (2), the enzyme B is a mixture of candida cylindracea lipase and rhizomucor miehei lipase.
  5. 5. The camellia seed oil diglyceride composition according to claim 1, wherein the preparation method of the cynanchum atratum extract is characterized in that the cynanchum atratum extract is prepared by crushing the cynanchum atratum rhizome, mixing with an extraction solvent, adding cellulase and pectase for enzymolysis, filtering to obtain filtrate, and concentrating, wherein the extraction solvent is a mixed solvent of glycerol, propylene glycol and water in a mass ratio of 0.06-0.09:0.3-0.5:1; the preparation method of the cornflower extract comprises pulverizing cornflower powder, mixing with eutectic solvent (DES solvent), ultrasonic extracting, and purifying with macroporous resin, wherein the eutectic solvent is a mixed solution of choline chloride and propylene glycol with a molar ratio of 1:1.5-2.2; The preparation method of kava root extract comprises pulverizing kava root, extracting with ethanol, eluting with macroporous adsorbent resin column, eluting with 65-70% ethanol water solution, collecting eluate, performing nanofiltration with molecular weight cut-off of 500Da, collecting permeate, concentrating, and drying.
  6. 6. The method for preparing the camellia seed oil diglyceride composition according to any one of claims 1 to 5, which is characterized by comprising the step of mixing the raw materials.
  7. 7. An eye patch characterized in that the raw materials comprise the oil tea seed oil diglyceride composition as claimed in any one of claims 1 to 5 and auxiliary materials.
  8. 8. The eye patch of claim 7, wherein the auxiliary material comprises a solvent, a humectant, a thickening agent, a pH regulator and a solubilizing agent, wherein the solvent is water, the humectant is at least one selected from glycerol, propylene glycol, dipropylene glycol, methyl propylene glycol, betaine, 1, 2-hexanediol, butanediol, trehalose, erythritol, sorbitol, panthenol, allantoin, sodium hyaluronate, hydrolyzed hyaluronic acid, tremella polysaccharide, beta-glucan or sodium polyglutamate, the thickening agent is at least one selected from carbomer, xanthan gum, guar gum, acacia gum, hydroxyethyl cellulose or hydroxypropyl methyl cellulose, the pH regulator is at least one selected from aminomethylpropanol, citric acid, sodium dihydrogen phosphate or tromethamine, and the solubilizing agent is at least one selected from PEG-40 hydrogenated castor oil, polysorbate 80, polysorbate 20 or coco glucoside.
  9. 9. The eye patch of claim 7, wherein the mass ratio of the camellia seed oil diglyceride composition to the auxiliary material is 15-25:75-85.
  10. 10. A method of preparing an eye patch according to any one of claims 7 to 9, comprising the steps of: s1, mixing a humectant, a thickener and 30% -60% of a formula amount of a solvent to obtain a mixture 1; S2, mixing the oil tea seed oil diglyceride composition with the residual solvent to obtain a mixture 2; and S3, mixing the mixture 1, the mixture 2, the pH regulator and the solubilizer, and filtering to obtain the aqueous emulsion.

Description

Oil tea seed oil diglyceride composition capable of relieving, removing wrinkles, removing black and improving eyesight, eye mask and preparation method thereof Technical Field The invention relates to the technical field of eye patches, in particular to a camellia seed oil diglyceride composition for relieving, removing wrinkles, removing black and improving eyesight, an eye patch and a preparation method thereof. Background The eye periphery is the weakest area of human skin, the total thickness of epidermis and dermis is only 0.25-0.55mm, sebaceous glands, sweat glands and sufficient collagen and elastic fiber support are lacking under the skin, and tens of thousands of blinking movements are needed daily, so that the area is extremely easy to be influenced by external stimulus and aging, meanwhile, factors such as popularization of video terminals, irregular work and rest and the like in modern life are superimposed, and the eye problems present multidimensional concurrency characteristics. In particular, the eye core trouble faced by the current consumer comprises four major types, namely a sensitive stimulation problem, abundant and fragile barrier of micro-blood vessels around eyes, discomfort such as redness, stinging, dryness and the like easily caused by environmental stimulation and stimulation of efficacy components, particularly prominent sensitive muscle groups, an aging wrinkle problem, quick loss of elastic fibers of skin around eyes, coexistence of dynamic lines and static lines, always existence of stimulation and efficacy imbalance of traditional wrinkle resistant components, a pigmentation problem, a problem caused by abnormal deposition of melanin, pigmentation or unsmooth circulation after inflammation of black eyes (containing pigments and blood vessels), a problem that conventional whitening components are difficult to combine mildness and targeting, a visual fatigue problem, eye dryness, eye distension, blurred vision and other visual fatigue symptoms caused by long-term eyes, and a problem of frequent synchronization with the skin around eyes, and a solution for improving double problems at the same time. The prior art discloses solutions to the aforementioned periocular problems, mostly eye patches, vapor masks, eye drops, eye creams, etc., but mostly address one or both of them. The preparation method comprises the steps of 1, taking fructus forsythiae, glossy privet fruit, chamomile, mulberry leaf, peppermint, dried rehmannia root, selfheal, spina date seed and polygala tenuifolia, mixing, adding water, sequentially decocting, cooling, filtering, concentrating and sterilizing to obtain the traditional Chinese medicine active ingredients, 2, taking powdered sodium alginate, adding water, heating and stirring to obtain a phase A solution, sequentially adding gelatin, methylparaben and glycerin into water, heating and stirring to obtain a mixed solution, then adding sorbitol, continuously heating and stirring to obtain a phase B solution, respectively standing the phase A solution and the phase B solution, uniformly mixing to obtain hydrogel, 3, adding the traditional Chinese medicine active ingredients into the hydrogel, uniformly stirring to obtain the hydrogel containing the traditional Chinese medicine active ingredients, pouring into an eye patch mould, dripping a cross-linking agent solution, refrigerating, standing, and demoulding to obtain the traditional Chinese medicine eye patch, so that the traditional Chinese medicine eye patch can effectively relieve the fatigue of vision and improve eyesight. The Chinese patent application CN107551031A provides a traditional Chinese medicine composition for relieving eye fatigue and an eye mask, wherein chrysanthemum indicum, concha haliotidis and Huang Baigong are taken as monarch drugs, chrysanthemum indicum has the effects of clearing heat and detoxicating, clearing liver and improving vision, concha haliotidis has the effects of calming liver and astringing gall, calming liver and suppressing yang, phellodendron amurense has the effects of calming liver and improving vision, the chrysanthemum indicum, concha haliotidis and phellodendron amurense are compatible, the effects of calming liver and improving vision are synergistically improved, selfheal and cortex moutan are taken as ministerial drugs, the selfheal has the effects of clearing fire and improving vision, resolving masses and detumescence, the cortex moutan has the effects of resisting bacteria, diminishing inflammation and easing pain, the selfheal, cortex moutan and the monarch drugs are compatible, the effects of clearing liver and improving vision, detumescence and anti-inflammation are taken as adjuvant, the salvia miltiorrhiza, borneol and menthol have the effects of activating blood and removing stasis, borneol and menthol have the effects of inducing resuscitation, resolving stagnated fire and relieving pain, the effects of all drugs are combined, so that the dru