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CN-121971346-A - Agilawood hydrolat-nicotinamide compound toner with antioxidation effect and preparation process thereof

CN121971346ACN 121971346 ACN121971346 ACN 121971346ACN-121971346-A

Abstract

The invention relates to the technical field of toner preparation, in particular to agilawood hydrosol-nicotinamide composite toner with an antioxidant effect, which comprises the following raw materials in parts by weight: 25.9 to 34.9 parts of deionized water, 60 to 65 parts of modified agilawood base solution, 3 to 5 parts of nano lipid modified nicotinamide, 2 to 4 parts of anti-repair compound solution and 0.1 part of 0.1 percent disodium ethylenediamine tetraacetate solution; according to the invention, the agilawood truffle active ingredient is kept stable by using the modified agilawood base solution, and the effects of antioxidation and anti-aging are cooperated, the stability of the nicotinamide active ingredient is improved and the skin irritation is reduced by modifying the nicotinamide with nano lipid, and the synergic effect and coexistence of the antioxidation effect and the barrier repair effect on the skin are realized by the anti-repair liquid.

Inventors

  • YAN XIAOMAO

Assignees

  • 瑜丰沉香汇(广东)科技有限公司

Dates

Publication Date
20260505
Application Date
20260401

Claims (10)

  1. 1. The agilawood hydrosol-nicotinamide composite toner with the antioxidation effect is characterized by comprising, by weight, 25.9-34.9 parts of deionized water, 60-65 parts of modified agilawood base solution, 3-5 parts of nano lipid modified nicotinamide, 2-4 parts of anti-repair composite solution and 0.1 part of 0.1% disodium ethylenediamine tetraacetate solution; the preparation method of the agilawood hydrolat-nicotinamide composite toner with the antioxidation effect comprises the following steps: s1, adding deionized water and 0.1% of ethylene diamine tetraacetic acid solution, stirring for 5 minutes at normal temperature, adding the modified agilawood base solution, and continuously stirring for 10 minutes to form uniform base solution; S2, sequentially adding nano lipid modified nicotinamide and anti-repair compound liquid into the base liquid, and stirring for 15 minutes to obtain a mixed solution; S3, regulating the pH value of the mixed solution, and filtering after ultrasonic treatment to obtain the agilawood hydrolat-nicotinamide compound toner with an antioxidant effect.
  2. 2. The method for preparing the agilawood truffle-nicotinamide composite toner with the anti-oxidation effect according to claim 1, wherein the preparation method comprises the steps of taking agilawood truffle, adding food-grade diatomite, stirring, standing for 20 minutes, adopting a polyethersulfone filter membrane for vacuum filtration, collecting purified agilawood truffle filtrate, adding deionized water into the purified agilawood truffle filtrate, increasing the temperature of the purified agilawood truffle filtrate, adding 1, 2-hexanediol, stirring for 15 minutes, adding p-hydroxyacetophenone, continuing stirring for 10 minutes, forming uniform anti-corrosion base solution, cooling the anti-corrosion base solution, adding ergothioneine, stirring for 8 minutes, adding 10% acetyl hexapeptide-8 solution, stirring for 5 minutes at a low speed, adjusting the pH value, conducting ultrasonic treatment for 10 minutes, and conducting secondary filtration through a filter membrane to obtain the modified base solution.
  3. 3. The agalloch eaglewood hydrol-nicotinamide compound toner with an antioxidant effect according to claim 2, wherein the mass ratio of the agalloch eaglewood hydrol to the food-grade diatomite is 2000:1, the mass ratio of the purified agalloch eaglewood hydrol filtrate to deionized water is 280:113, the mass ratio of the purified agalloch eaglewood hydrol filtrate to 1, 2-hexanediol is 70:1, and the mass ratio of the purified agalloch eaglewood hydrol filtrate to p-hydroxyacetophenone is 140:1.
  4. 4. The agilawood hydrolat-nicotinamide composite toner with anti-oxidation effect according to claim 2, wherein the mass ratio of the antiseptic base solution to ergothioneine is 1995:1, and the mass ratio of the antiseptic base solution to 10% acetyl hexapeptide-8 solution is 1995:4.
  5. 5. The method for preparing the agilawood hydrolat-nicotinamide compound toner with the anti-oxidation effect is characterized in that the preparation method comprises the steps of adding soybean lecithin, cholesterol and vitamin E into a round-bottom flask, pouring absolute ethyl alcohol into the round-bottom flask, stirring for 30 minutes to form a transparent lipid solution, starting a rotary evaporator, controlling the temperature, evaporating for 30 minutes, taking nicotinamide, adding deionized water into the solution, stirring to form an aqueous solution of nicotinamide, pouring the aqueous solution of nicotinamide into the round-bottom flask, keeping the temperature of a water bath, stirring to form a liposome suspension, transferring the liposome suspension to a high-pressure homogenizer, ultrafiltering the liposome solution through an ultrafiltration membrane at normal temperature, and adjusting the pH value to obtain the nanometer lipid modified nicotinamide.
  6. 6. The aquilaria sinensis hydrolat-nicotinamide composite toner with an antioxidant effect according to claim 5, wherein the mass ratio of soybean lecithin, cholesterol, vitamin E and absolute ethyl alcohol is 600:200:1:600, and the mass ratio of nicotinamide to deionized water is 2:1.
  7. 7. The aquilaria sinensis hydrolat-nicotinamide compound toner with an antioxidant effect according to claim 5, wherein the mass ratio of the nicotinamide aqueous solution to the transparent lipid solution is 600:1401.
  8. 8. The method for preparing the anti-repair compound liquid comprises the steps of adding polyethylene glycol 400 into a reaction kettle, heating and stirring, adding xanthan gum, continuously stirring for 15 minutes, slowly adding ceramide NP, maintaining the temperature, increasing the stirring speed for 40 minutes, forming a transparent fat-soluble base liquid, taking deionized water, adding ascorbyl glucoside into the deionized water at normal temperature, stirring for 10 minutes to obtain an ascorbyl glucoside aqueous solution, pouring the ascorbyl glucoside aqueous solution into the fat-soluble base liquid, maintaining the temperature for 30 minutes, forming an oil-water mixed solution, starting ultrasonic equipment, performing ultrasonic treatment on the oil-water mixed solution for 20 minutes to form a transparent solution, cooling the transparent solution, reducing the stirring speed, maintaining the temperature for 15 minutes, adjusting the pH value, and filtering with a polytetrafluoroethylene filter membrane to obtain an anti-repair compound liquid.
  9. 9. The agilawood hydrolat-nicotinamide compound toner with anti-oxidation effect according to claim 8, wherein the mass ratio of polyethylene glycol 400 to xanthan gum to ceramide NP is 250:1:50, the mass ratio of deionized water to ascorbyl glucoside is 13:3, and the mass ratio of ascorbyl glucoside aqueous solution to fat-soluble base solution is 1:1.
  10. 10. The agilawood hydrolat-nicotinamide composite toner with anti-oxidation effect according to claim 1, wherein the mass ratio of deionized water to 0.1% disodium edetate solution is 304:1, the mass ratio of modified agilawood base solution to deionized water is 625:304, and the mass ratio of base solution to nanometer lipid modified nicotinamide to anti-repair composite solution is 93:4:3.

Description

Agilawood hydrolat-nicotinamide compound toner with antioxidation effect and preparation process thereof Technical Field The invention relates to the technical field of toner preparation, in particular to agilawood hydrolat-nicotinamide compound toner with an antioxidant effect and a preparation process thereof. Background The toner is a liquid skin care product which is used immediately after the cleansing of the face and is a foundation for subsequent maintenance, and has the core effects of carrying out mild secondary cleaning, removing possible residual impurities, helping the skin to quickly recover to a healthy weak acid state, relieving the tight feel after the cleansing of the face, simultaneously, supplementing moisture for the stratum corneum immediately, softening the skin, remarkably improving the permeation and absorption efficiency of subsequent essence and emulsion products, forming a complete and efficient skin care closed loop, and enabling the skin to reach an ideal state of moisture and balance. The prior art for preparing the toner containing the agilawood truffle and the nicotinamide generally adopts a simple mixing process, the agilawood truffle is prepared by a high-temperature steam distillation method, then the agilawood truffle and common nicotinamide powder are subjected to physical stirring and mixing at room temperature, but the prior art for preparing the toner can cause degradation of sesquiterpenes active components in the agilawood truffle in the high-temperature distillation process, so that the antioxidation effect is influenced, the antiseptic property is poor, the ecological balance of skin can be damaged after long-term use, the problem of irritation and sensitivity to the skin is solved, the common nicotinamide is added, the effect is easy to fade in the shelf life, the stability is poor, the nicotinamide is easy to decompose and lose efficacy is easy to lose efficacy to partial skin, the simple mixing can not enable the agilawood truffle component and the nicotinamide component to coexist, the two effects of antioxidation and barrier repair of the toner on the skin can not be synergistically exerted, and the components of the toner are easy to lose efficacy. Based on the above, the application provides the agilawood hydrolat-nicotinamide compound toner with an antioxidant effect and a preparation process thereof. Disclosure of Invention The invention aims to provide agilawood hydrolat-nicotinamide compound toner with an antioxidant effect and a preparation process thereof, and the agilawood hydrolat-nicotinamide compound toner with the antioxidant effect has stable and efficient antioxidant and anti-aging effects, reduces skin irritation, promotes active ingredients to be absorbed by skin, and realizes synergistic effect of antioxidant and skin barrier repair. In order to achieve the above object, the present invention provides the following technical solutions: the agilawood hydrosol-nicotinamide composite toner with the antioxidation effect comprises, by weight, 25.9-34.9 parts of deionized water, 60-65 parts of modified agilawood base solution, 3-5 parts of nano lipid modified nicotinamide, 2-4 parts of anti-repair composite solution and 0.1 part of 0.1% disodium ethylenediamine tetraacetate solution; the preparation method of the agilawood hydrolat-nicotinamide composite toner with the antioxidation effect comprises the following steps: S1, adding deionized water and 0.1% disodium ethylenediamine tetraacetate solution, stirring at normal temperature at 300rpm for 5 minutes, adding the modified agilawood base solution, and continuously stirring for 10 minutes to form uniform base solution; s2, sequentially adding nano lipid modified nicotinamide and anti-repair liquid into the base liquid, and stirring at a rotation speed of 250rpm for 15 minutes to obtain a mixed solution, and fusing the anti-oxidation and anti-aging functions; S3, adding citric acid into the mixed solution to adjust the pH value to 5.5-6.5, performing ultrasonic treatment at 20kHz for 5 minutes, and filtering with a 0.45 mu m filter membrane to obtain the agilawood truffle-nicotinamide compound toner with an antioxidant effect. The preparation method comprises the steps of selecting high-quality agilawood with oil content more than or equal to 15%, removing impurities, crushing into small blocks, cleaning, airing, placing into a sealed distillation device, purifying to obtain agilawood raw juice, adding food-grade diatomite, stirring at 300rpm, standing for 20 minutes, adsorbing suspended impurities and partial microorganisms through diatomite, adopting a 0.22 mu m polyether sulfone filter membrane for vacuum filtration, collecting purified agilawood pure dew filtrate for later use, avoiding the influence of impurities on the subsequent anti-corrosion effect, adding deionized water into the purified agilawood pure dew filtrate, stirring uniformly, heating the purified agilawood pure dew filtrate