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CN-121987534-A - Preparation method of matsutake water supplementing and moisturizing essence

CN121987534ACN 121987534 ACN121987534 ACN 121987534ACN-121987534-A

Abstract

The application relates to the technical field of cosmetics, and particularly discloses a preparation method of a matsutake moisturizing essence. The preparation method comprises the following steps of S1, cleaning fresh matsutake to obtain clean matsutake, S2, crushing the clean matsutake to obtain matsutake particles, S3, extracting the matsutake particles to obtain matsutake cell stock solution, S4, carrying out constant-temperature stirring treatment on the matsutake cell stock solution to obtain primary composite solution, S5, adding a composite preservative into the primary composite solution, carrying out vacuum stirring and directional filtering to obtain stable mixed solution, S6, standing the stable mixed solution to obtain curing solution, S7, filling the curing solution to obtain a filling product, S8, sterilizing the filling product to obtain a sterilized product, and S9, packaging. The preparation method can be used for preparing high-end skin care essence products with high activity and high stability, and has the advantages of retaining natural active ingredients of tricholoma matsutake, ensuring long-acting stability of the products, and improving skin feel and absorption efficiency in use.

Inventors

  • HAO YANWEI

Assignees

  • 青岛东临栈桥科技发展有限公司

Dates

Publication Date
20260508
Application Date
20260305

Claims (10)

  1. 1. The preparation method of the matsutake moisturizing essence is characterized by comprising the following steps of: s1, cleaning fresh tricholoma matsutake serving as a raw material to obtain clean tricholoma matsutake; s2, carrying out low-temperature crushing treatment on the cleaned tricholoma matsutake obtained in the step S1 under the protection of inert gas to obtain tricholoma matsutake particles; S3, adding a biological enzymolysis agent into the tricholoma matsutake particles obtained in the step S2, and then performing low-temperature enzymolysis extraction to obtain tricholoma matsutake cell stock solution; s4, adding a natural moisturizing factor compound into the tricholoma matsutake cell stock solution obtained in the step S3, and stirring at constant temperature to obtain a primary compound solution; S5, adding a composite preservative into the preliminary composite liquid obtained in the step S4 in stages, and carrying out directional filtration after vacuum stirring treatment to obtain a stable mixed liquid; s6, carrying out gradient standing treatment on the stable mixed solution obtained in the step S5 in an oxygen-controlled environment to obtain a curing solution; s7, filling the curing liquid obtained in the step S6 in a sterile environment to obtain a filling product; S8, performing pulsed light synergistic low-temperature sterilization treatment on the filling product obtained in the step S7 to obtain a sterilized product; And S9, packaging the sterilized product of S8 under inert atmosphere to obtain the high-activity matsutake moisturizing essence.
  2. 2. The method for preparing the tricholoma matsutake moisturizing essence according to claim 1, wherein the method further comprises the step of pretreating the fresh tricholoma matsutake before the step S1, wherein the fresh tricholoma matsutake after picking is transported in a low-temperature environment of 0-4 ℃ and the pretreatment is completed within 2 hours.
  3. 3. The method for preparing a moisturizing essence according to claim 1, wherein in step S2, the low-temperature crushing treatment is performed in an environment of-10 ℃ to 0 ℃ and the particle size of the matsutake particles is controlled to be 0.3 mm to 0.7mm.
  4. 4. The method for preparing the matsutake moisturizing essence according to claim 1, wherein in the step S3, the biological enzymolysis agent comprises cellulase, pectase and-glucanase, the enzymolysis temperature is controlled to be 35-45 ℃, the pH value is maintained to be 5.0-6.0, and the enzymolysis time is 2-4 hours.
  5. 5. The method for preparing the matsutake water-replenishing and moisturizing essence according to claim 1, wherein in the step S4, the natural moisturizing factor compound comprises sodium hyaluronate, trehalose and matsutake polysaccharide, the total amount of the added sodium hyaluronate, trehalose and matsutake polysaccharide is 3-8% of the mass of the primary compound, the temperature of the constant-temperature stirring treatment is controlled at 35-45 ℃, and the stirring time is 40-60 minutes.
  6. 6. The method for preparing the matsutake moisturizing essence according to claim 1, wherein in the step S5, the compound preservative comprises phenoxyethanol, chlorphenesin and natural antibacterial peptide, the vacuum degree of the vacuum stirring treatment is maintained at-0.06 to-0.08 MPa, the temperature is 35-45 ℃ and the time is 50-70 minutes, and the total bacterial count of the stable mixed solution is controlled to be 10CFU/mL by directional filtration.
  7. 7. The method for preparing a moisturizing essence according to claim 1, wherein in step S6, the gradient standing treatment comprises standing for 30-40 minutes at 15-25 ℃ and then standing for 20-30 minutes at 5-10 ℃.
  8. 8. The method for preparing the matsutake moisturizing essence according to claim 1, wherein in the step S7, the filling process is performed in a sterile environment with an oxygen content of 0.1%.
  9. 9. The method for preparing the matsutake moisturizing essence according to claim 1, wherein in the step S8, the pulsed light is used together with low-temperature sterilization, and the pulsed light is irradiated for 10-20 seconds by using pulsed light with the wavelength of 200-300nm, and then the temperature is kept at 60-70 ℃ for 20-30 minutes.
  10. 10. The method for preparing the matsutake moisturizing essence according to claim 1, wherein in the step S9, the encapsulation process is performed in an inert atmosphere environment with an oxygen content of less than 0.5%, the ambient temperature during encapsulation is controlled to be 15-25 ℃, the relative humidity is maintained to be 30-50%, and the low-temperature stabilization treatment is performed for 24 hours at 2-8 ℃ after the encapsulation is completed.

Description

Preparation method of matsutake water supplementing and moisturizing essence Technical Field The application relates to the technical field of cosmetics, in particular to a preparation method of a matsutake moisturizing essence. Background The moisturizing essence is used as an important component in a skin care process, is usually used after cleansing and using toner, before smearing emulsion or cream, and rapidly permeates muscle bottoms by virtue of a small molecular structure and high-concentration active ingredients, so that the moisturizing essence can efficiently supplement and lock moisture, not only immediately relieve dryness and tightness, but also strengthen skin barriers, improve the absorption capacity of subsequent maintenance products, improve skin quality after long-term use, keep the skin moist, soft and smooth, and assist a user to cope with situations of environmental dryness, air-conditioning environment and insufficient moisturizing capacity. The related moisturizing essence realizes the moisturizing function by compounding a chemical synthetic humectant and a plant extract, but the adopted extraction process and production flow are easy to destroy the active structure of thermosensitive natural raw materials such as tricholoma matsutake and the like, and meanwhile, the conventional preservative and emulsifier added for maintaining the stability of the system can interfere with the active ingredients, so that the natural active ingredients are inactivated and the stability of the product is insufficient. Disclosure of Invention The application provides a preparation method of a matsutake moisturizing essence, which aims to solve the problems of inactivation of natural active ingredients and insufficient product stability caused by compounding of a related moisturizing essence with a plant extract through a chemical synthesis humectant. The application provides a preparation method of a matsutake moisturizing essence, which adopts the following technical scheme: A preparation method of a matsutake moisturizing essence comprises the following steps: s1, cleaning fresh tricholoma matsutake serving as a raw material to obtain clean tricholoma matsutake; s2, carrying out low-temperature crushing treatment on the cleaned tricholoma matsutake obtained in the step S1 under the protection of inert gas to obtain tricholoma matsutake particles; S3, adding a biological enzymolysis agent into the tricholoma matsutake particles obtained in the step S2, and then performing low-temperature enzymolysis extraction to obtain tricholoma matsutake cell stock solution; s4, adding a natural moisturizing factor compound into the tricholoma matsutake cell stock solution obtained in the step S3, and stirring at constant temperature to obtain a primary compound solution; S5, adding a composite preservative into the preliminary composite liquid obtained in the step S4 in stages, and carrying out directional filtration after vacuum stirring treatment to obtain a stable mixed liquid; s6, carrying out gradient standing treatment on the stable mixed solution obtained in the step S5 in an oxygen-controlled environment to obtain a curing solution; s7, filling the curing liquid obtained in the step S6 in a sterile environment to obtain a filling product; S8, performing pulsed light synergistic low-temperature sterilization treatment on the filling product obtained in the step S7 to obtain a sterilized product; And S9, packaging the sterilized product of S8 under inert atmosphere to obtain the high-activity matsutake moisturizing essence. By adopting the technical scheme, the fresh tricholoma matsutake surface dirt and microorganisms are cleaned and removed in the step S1, a cleaning basis is provided for the subsequent steps, the low-temperature crushing of the S2 under inert gas minimizes oxidation reaction, biological activity of the tricholoma matsutake is kept, and a proper particle size is provided for enzymolysis of the S3, then the biological enzymolysis of the S3 utilizes specific enzymes to decompose cell walls and release internal moisture retention components, the natural moisture retention factor compound added in the S4 and the tricholoma matsutake stock solution synergistically enhance moisture absorption and retention capacity, then the staged preservative addition and vacuum stirring of the S5 inhibit microorganism growth while removing bubbles, the product stability is improved, the gradient standing of the S6 promotes intermolecular interaction through temperature change, the texture is improved, the aseptic filling of the S7 can prevent secondary pollution, the pulse light of the S8 synergistically kills pathogens at low temperature effectively without damaging thermosensitive components, and finally the inert atmosphere of the S9 seals oxygen contact, so that the quality guarantee period is prolonged, and the pine essence product with high activity, strong moisture retention and safety and stability