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CN-121991772-A - Ampelopsis grossedentata essential oil washing soap based on high-frequency extraction Ampelopsis grossedentata stock solution and preparation method thereof

CN121991772ACN 121991772 ACN121991772 ACN 121991772ACN-121991772-A

Abstract

The application relates to the technical field of washing and protecting soaps, and particularly discloses a vine tea essential oil washing and protecting soap based on high-frequency extraction vine tea stock solution and a preparation method thereof. A vine tea essential oil washing and protecting soap based on high-frequency extraction of vine tea stock solution is prepared from the following raw materials in parts by weight, namely vine tea stock solution, sodium hydroxide, vine tea essential oil, fructus psoraleae essential oil, fructus cnidii essential oil, cortex dictamni essential oil, green tea seed and olive small molecular oil, mango kernel small molecular oil, palm oil and coconut small molecular oil, wherein the preparation method comprises the steps of S1, vine tea stock solution preparation, S2, alkali solution preparation, S3, oil phase mixing and saponification, S4, defoaming and forming. The vine tea essential oil washing and caring soap based on the high-frequency extraction vine tea stock solution can be used for various personal care scenes such as daily facial cleaning, body bathing and scalp nursing, and has the advantages of high active ingredient retention rate, good balance degree of cleaning force and mildness, synergistic effect of plant essential oil and good product stability.

Inventors

  • Tian Miyuan

Assignees

  • 来凤酉味生物科技有限责任公司

Dates

Publication Date
20260508
Application Date
20260126

Claims (10)

  1. 1. The vine tea essential oil washing and protecting soap is characterized by being prepared from the following raw materials, by weight, 40-60 parts of vine tea stock solution, 40-60 parts of sodium hydroxide, 4-6 parts of vine tea essential oil, 1-4 parts of fructus psoraleae essential oil, 1-4 parts of cnidium essential oil, 1-4 parts of cortex dictamni essential oil, 20-30 parts of green tea seed olive small molecular oil, 4-9 parts of mango kernel small molecular oil, 2-6 parts of palm oil and 8-12 parts of coconut small molecular oil.
  2. 2. The vine tea essential oil washing soap based on the high-frequency extraction vine tea stock solution, which is disclosed in claim 1, is characterized in that the weight ratio of the vine tea stock solution to sodium hydroxide is 1:1.
  3. 3. The vine tea essential oil washing soap based on the high-frequency extraction vine tea stock solution, according to claim 1, wherein the addition amount of the vine tea essential oil is 3% of the total weight of the washing soap.
  4. 4. The vine tea essential oil washing soap based on the high-frequency extraction vine tea stock solution, according to claim 1, wherein the sum of the adding amount of the fructus psoraleae essential oil and the fructus cnidii essential oil accounts for 5% of the total weight of the washing soap.
  5. 5. The vine tea essential oil washing soap based on the high-frequency extraction vine tea stock solution, according to claim 1, wherein the sum of the addition amount of the green tea seed small molecular oil and the mango kernel small molecular oil accounts for 65% of the total weight of the washing soap.
  6. 6. The vine tea essential oil washing soap based on the high-frequency extraction vine tea stock solution, according to claim 1, wherein the sum of the addition amounts of palm oil and coconut small molecule oil accounts for 26% of the total weight of the washing soap.
  7. 7. The preparation method of the vine tea essential oil washing and protecting soap based on the high-frequency extraction vine tea stock solution is characterized by comprising the following steps of: S1, preparing vine tea stock solution, namely taking fresh vine tea, adopting a high-frequency extraction device, and condensing cell liquid at 55-65 ℃ to 19-30 ℃ under the action of a compressor through a condensation pipeline within 75-115 minutes of extraction time to obtain vine tea stock solution; S2, preparing alkali liquor, namely pre-freezing the vine tea stock solution obtained in the step S1 into ice cubes, mixing the ice cubes with sodium hydroxide according to the weight ratio of 1:1, and then cooling the ice cubes to below 44 ℃ to obtain the alkali liquor; S3, mixing and saponifying the oil phase, namely sequentially adding part of vine tea essential oil, fructus psoraleae essential oil, fructus cnidii essential oil, cortex dictamni essential oil, green tea seed and olive small molecular oil, mango kernel small molecular oil, palm oil and coconut small molecular oil into the alkali liquor obtained in the step S2, controlling the temperature of the soap liquor in the adding process, and stirring in a segmented manner until the soap liquor is smooth; And S4, defoaming and forming, namely adding residual vine tea essential oil into the silky soap solution obtained in the step S3 again, vacuumizing and defoaming, putting the soap solution into a mold after no bubbles exist in the soap solution, standing for 24 hours, demolding, and dividing the soap solution into blocks to obtain the vine tea essential oil soap.
  8. 8. The preparation method of the vine tea essential oil washing and protecting soap based on the high-frequency extraction vine tea stock solution, which is characterized by comprising the steps of adding vine tea essential oil and fructus psoraleae essential oil for the first time, stirring for 3 hours, adding fructus cnidii essential oil for the second time, stirring for 2 hours, adding cortex dictamni essential oil for the third time, adding green tea seed small molecule oil for the fourth time, stirring for 2 hours, adding mango seed small molecule oil for the fifth time, stirring for 20 minutes, adding palm oil for the sixth time, stirring for 1 hour, adding coconut small molecule oil for the seventh time, and stirring for 1 hour, wherein the temperature of the first 4 oiling soap solutions is controlled within 17 ℃ and the temperature of the last 3 times is controlled within 22 ℃.
  9. 9. The method for preparing vine tea essential oil washing soap based on high-frequency extraction vine tea stock solution according to claim 7, wherein in the step S4, parameters of vacuumizing and defoaming treatment are that the vacuumizing time is set to be within 15 minutes, and the pressure maintaining time is set to be 20 minutes.
  10. 10. The method for preparing vine tea essential oil washing soap based on high-frequency extraction vine tea stock solution according to claim 7, wherein in the step S4, the weight of the vine tea essential oil added again is 66% of the total weight of the vine tea essential oil.

Description

Ampelopsis grossedentata essential oil washing soap based on high-frequency extraction Ampelopsis grossedentata stock solution and preparation method thereof Technical Field The application relates to the technical field of washing and protecting soaps, in particular to a vine tea essential oil washing and protecting soap based on high-frequency extraction vine tea stock solution and a preparation method thereof. Background The washing and caring soap is a solid soap-like product with the functions of cleaning and nursing, is mainly prepared by taking fatty acid salt as a core cleaning component through saponification reaction, and is widely used for cleaning and nursing human skin, hair and specific fabrics; the skin-cleaning agent has the core characteristics that firstly, in addition to basic cleaning components, nursing components such as humectant, plant extracts and vitamins are often added, dirt and grease are cleaned, skin dryness is reduced, secondly, in application scenes, the skin-cleaning agent can be subdivided into facial soap, bath soap, shampoo soap, underwear soap and the like, the cleaning requirements of different parts or objects are met, thirdly, in the use characteristics, foam is rich, washing is easy, and part of products can adjust the formula according to different skin types such as sensitive muscles and oily muscles, so that cleaning force and mildness are balanced. The related washing and caring soap improves the functional diversity of the product by adding the conventional plant extract or essential oil component, but the extraction process often causes a great deal of loss of heat-sensitive active components due to high temperature or long-time treatment, meanwhile, the simple physical mixing of the functional components is difficult to generate effective synergistic effect, and the incomplete or oversaponification of the saponification reaction is easily caused by inaccurate alkali amount proportioning control, so that the content of the active components of the product is insufficient, the comprehensive maintenance effect is poor and the stability is reduced. Disclosure of Invention In order to solve the problems of insufficient content of active ingredients, poor comprehensive maintenance effect and reduced stability of products caused by adding conventional plant extracts or essential oil components into relevant washing and caring soaps, the application provides a vine tea essential oil washing and caring soap based on high-frequency extraction vine tea stock solution and a preparation method thereof. In a first aspect, the application provides a vine tea essential oil washing soap based on high-frequency extraction vine tea stock solution, which adopts the following technical scheme: a vine tea essential oil washing and protecting soap based on high-frequency extraction of vine tea stock solution is prepared from the following raw materials, by weight, 40-60 parts of vine tea stock solution, 40-60 parts of sodium hydroxide, 4-6 parts of vine tea essential oil, 1-4 parts of fructus psoraleae essential oil, 1-4 parts of fructus cnidii essential oil, 1-4 parts of cortex dictamni essential oil, 20-30 parts of green tea seed and olive small molecule oil, 4-9 parts of mango kernel small molecule oil, 2-6 parts of palm oil and 8-12 parts of coconut small molecule oil. According to the technical scheme, the formula system of the washing soap takes vine tea stock solution obtained by high-frequency extraction as a water phase matrix, active flavonoid compounds contained in the vine tea stock solution are subjected to saponification reaction with sodium hydroxide to form a cleaning base, the compound combination of vine tea essential oil, fructus psoraleae essential oil, fructus cnidii essential oil and cortex dictamni essential oil synergistically plays roles in relieving and cleaning, meanwhile, high-proportion unsaponifiable matters such as green tea seed olive small molecular oil, mango kernel small molecular oil and the like are reserved in a soap body as natural moisturizing components, and palm oil and coconut small molecular oil are used for providing foamability and hardness, so that a solid washing product with cleaning, maintenance and relieving functions can be provided. Preferably, the weight ratio of the vine tea stock solution to the sodium hydroxide is 1:1. Through adopting above-mentioned technical scheme, control alkali lye concentration can ensure that the saponification reaction is complete, and this one-to-one weight portion proportional relation makes the sodium hydroxide can fully react with the acidic component in grease and vine tea stoste, and then avoids having free alkali to lead to skin irritation in the finished product, prevents not completely saponification simultaneously to influence product quality. Preferably, the addition amount of the vine tea essential oil accounts for 3% of the total weight of the washing soap. By adopting the technical sche